SAND - Small-Angle Neutron Diffractometer

Instrument Scientist - P. Thiyagarajan (Thiyaga)
Engineering Associate - Denis G. Wozniak
Post Docs - Sai Venkatesh Pingali
Click Here for the SAND Run Schedule
SAND is a time-of-flight Small-Angle Neutron Diffractometer at the IPNS facility at Argonne National Laboratory. This instrument is an improved version of SASI, in which a larger area detector, a wide angle Linear Position-Sensitive Detector bank, and larger sample-to-detector distance are used. This enables SAND to obtain higher quality data in a much wider Q range (0.0035 to 2 Å-1) in a single measurement. Currently, the LPSD bank is not yet installed which restricts the Q range into 0.0035 to 0.6 Å-1. As an example, data for a phase separated paraffin mixture are shown below.
At the BESSRC CAT of the Advanced Photon Source there is a SAXS Instrument that can do both time-resolved SAXS and Anomalous SAXS with a Q range of 0.003 - 0.8 inverse Angstroms. Furthermore, a SAXS facility is available on a rotating anode x-ray source which can access the Q region of 0.01 - 0.2 inverse Angstroms. This uses 20 cm x 20 cm gas detector. For further information, contact thiyaga@anl.gov.
| Beam Line |
C3 |
| Source Freqency |
30 Hz |
| Moderator |
Coupled 24K solid methane |
| Wavelength Range |
1 to 14 Å |
| Moderator-to-Sample Distance |
7.0 m |
| Sample-to-Area Detector Distance |
2.0 m |
| Sample-to-LPSD Distance |
1.524 m |
| Focusing Soller Collimators |
0.0034 radians FWHM |
| Beam Diameter at Moderator |
9.0 cm |
| Beam Diameter at Area Detector |
2.1 cm |
| Area Detector |
| Active Volume |
40 x 40 cm2, 2.5 cm thick |
| Resolution |
4 - 6 mm FWHM |
| Q Range |
0.0035 to 0.6 Å-1 |
| Q resolution (s (Q)/Q) |
0.3 to 0.023 |
| LPSD (65 Detectors) |
| Active Volume per Detector |
1.1 cm diameter x 60 cm long |
| Resolution |
1 - 2 cm along Detector |
| Q Range |
0.1 to 2 Å-1 |
| Ancillary Equipment |
| Sample Changer |
10 positions, 0 to 75 °C |
| Resistance Heater |
20 to 200 °C |
| Displex |
20 to 300 K |
| Pressure Cell |
1 to 2500 bar |
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