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SAND - Small-Angle Neutron Diffractometer

SAND

Instrument Scientist - P. Thiyagarajan (Thiyaga)
Engineering Associate - Denis G. Wozniak
Post Docs - Sai Venkatesh Pingali

Click Here for the SAND Run Schedule

SAND is a time-of-flight Small-Angle Neutron Diffractometer at the IPNS facility at Argonne National Laboratory. This instrument is an improved version of SASI, in which a larger area detector, a wide angle Linear Position-Sensitive Detector bank, and larger sample-to-detector distance are used. This enables SAND to obtain higher quality data in a much wider Q range (0.0035 to 2 Å-1) in a single measurement. Currently, the LPSD bank is not yet installed which restricts the Q range into 0.0035 to 0.6 Å-1. As an example, data for a phase separated paraffin mixture are shown below.

At the BESSRC CAT of the Advanced Photon Source there is a SAXS Instrument that can do both time-resolved SAXS and Anomalous SAXS with a Q range of 0.003 - 0.8 inverse Angstroms. Furthermore, a SAXS facility is available on a rotating anode x-ray source which can access the Q region of 0.01 - 0.2 inverse Angstroms. This uses 20 cm x 20 cm gas detector. For further information, contact thiyaga@anl.gov.

Beam Line C3
Source Freqency 30 Hz
Moderator Coupled 24K solid methane
Wavelength Range 1 to 14 Å
Moderator-to-Sample Distance 7.0 m
Sample-to-Area Detector Distance      2.0 m
Sample-to-LPSD Distance 1.524 m
Focusing Soller Collimators 0.0034 radians FWHM
Beam Diameter at Moderator 9.0 cm
Beam Diameter at Area Detector 2.1 cm
Area Detector
     Active Volume 40 x 40 cm2, 2.5 cm thick
     Resolution 4 - 6 mm FWHM
     Q Range 0.0035 to 0.6 Å-1
     Q resolution (s (Q)/Q) 0.3 to 0.023
LPSD (65 Detectors)
     Active Volume per Detector 1.1 cm diameter x 60 cm long
     Resolution 1 - 2 cm along Detector
     Q Range 0.1 to 2 Å-1
Ancillary Equipment
     Sample Changer 10 positions, 0 to 75 °C
     Resistance Heater 20 to 200 °C
     Displex 20 to 300 K
     Pressure Cell 1 to 2500 bar

May 31, 2006

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